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العنوان
Synthesis and characterization of nano coating by Sol - Gel technique and its analytical applications /
الناشر
Marwa Moustafa Elhusseiny ,
المؤلف
Marwa Moustafa Elhusseiny
هيئة الاعداد
باحث / Marwa Moustafa Elhusseiny
مشرف / Yousry M. Issa
مشرف / Nabil M. Amin
مناقش / Marwa Moustafa Elhusseiny
تاريخ النشر
2014
عدد الصفحات
107 P. :
اللغة
الإنجليزية
الدرجة
ماجستير
التخصص
Analytical Chemistry
تاريخ الإجازة
21/4/2015
مكان الإجازة
جامعة القاهرة - كلية العلوم - Analytical Chemistry
الفهرس
Only 14 pages are availabe for public view

from 172

from 172

Abstract

Titanium dioxide thin films have been synthesized by sol - gel spin coating technique on glass substrate. The prepared thin films have been submitted to different annealing temperature ranging from 300 upto 1000 {u00BA}C. The effects of annealing temperatures on the structural and optical properties of thin films were investigated. The films were characterized by different techniques: X - ray diffraction (XRD), UV - visible spectroscopy, scanning electron microscope (SEM) and transmission electron microscopy (TEM). The characterization studies revealed that the films are crystallized into nano - structured anatase and rutile phases. The mentioned data were confirmed by TEM, which revealed the presence of TiO₂ nano-particle of about (” " ~ " ”3 - 4 nm). The optical measurement showed the direct band gap. The TiO₂ thin films have higher transparency in the visible range at 100 {u00BA}C. SEM image of films annealed showed nano -crystalline structure of TiO₂ particles and they are approximately in spherical forms